Josland, Sam, and Oelgemöller, Michael (2014) Application Note 38: α-photodecarboxylation of phthaloyl glycine. Report. Vapourtec Ltd, Suffolk, UK.

PDF (Application Note) - Published Version Restricted to Repository staff only

Abstract

This application note illustrates the use of the Vapourtec UV-150 photochemical reactor for the conversion of phthaloyl glycine to N-methylphthalimide. The transformation has been systematically optimized in terms of reagent concentration and residence time. The optimized procedure was subsequently performed on large-scale, achieving a productivity of 1.15 g of product per hour (or 27.6 g per day). The reactor enabled continuous photochemistry in an easy-to-use, safe and efficient manner.

Item ID:	35705
Item Type:	Report (Report)
Keywords:	photochemistry; photodecarboxylation; flow chemistry; organic chemistry
Related URLs:	Publisher
Funders:	Australian Research Council (ARC)
Projects and Grants:	Discovery Project DP130100794
Date Deposited:	10 Jun 2015 04:57
FoR Codes:	03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030503 Organic Chemical Synthesis @ 60% 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030505 Physical Organic Chemistry @ 40%
SEO Codes:	97 EXPANDING KNOWLEDGE > 970103 Expanding Knowledge in the Chemical Sciences @ 100%
Downloads:	Total: 1
	More Statistics