A photochemical route for efficient cyclopeptide formation with a minimum of protection and activation chemistry
Griesbeck, Axel G., Heinrich, Thomas, Oelgemoeller, Michael, Lex, Johann, and Molis, Arne (2002) A photochemical route for efficient cyclopeptide formation with a minimum of protection and activation chemistry. Journal of the American Chemical Society, 124 (37). pp. 10972-10973.
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DOI: 10.1021/ja025804o
View at Publisher Website: http://dx.doi.org/10.1021/ja025804o
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Abstract
This protocol represents a new route for cyclopeptide formation with a minimum of protection and activation chemistry and is applied for more complex structures in ongoing work. These preliminary results suffer from medium chemical yields due to substantial hydrolysis at high pH, a competing process which can be suppressed using buffered aqueous conditions.
| Item ID: | 29744 |
|---|---|
| Item Type: | Article (Research - C1) |
| ISSN: | 1520-5126 |
| Date Deposited: | 08 Oct 2013 22:34 |
| FoR Codes: | 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030503 Organic Chemical Synthesis @ 40% 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030504 Organic Green Chemistry @ 30% 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030505 Physical Organic Chemistry @ 30% |
| SEO Codes: | 97 EXPANDING KNOWLEDGE > 970103 Expanding Knowledge in the Chemical Sciences @ 100% |
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