A SPE-LC-MS/MS method for the detection of low concentrations of pharmaceuticals in industrial waste streams
Deegan, Ann-Marie, Cullen, Mark , Oelgemoeller, Michael, Nolan, Kieran, Tobin, John, and Morrissey, Anne (2011) A SPE-LC-MS/MS method for the detection of low concentrations of pharmaceuticals in industrial waste streams. Analytical Letters, 44. pp. 2808-2820.
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Abstract
A SPE-LC-MS/MS method was developed and validated for the determination of three active pharmaceutical ingredients in the wastewater of a chemical synthesis production facility. The SPE-LC-MS/MS method was validated in actual influent and effluent samples. Linearity, LOD, LOQ, repeatability, intermediate precision, and recovery were determined. The LC-MS/MS method was used for an on-going monitoring program for these pharmaceuticals in wastewater. The method development techniques, validation procedures, and results from real wastewater samples are presented in this paper.
| Item ID: | 19361 |
|---|---|
| Item Type: | Article (Research - C1) |
| ISSN: | 1532-236X |
| Keywords: | mass spectrometry; pharmaceuticals; solid phase extraction; wastewater |
| Additional Information: | Corresponding author: michael.oelgemoeller@jcu.edu.au |
| Date Deposited: | 07 Dec 2011 04:56 |
| FoR Codes: | 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030599 Organic Chemistry not elsewhere classified @ 50% 03 CHEMICAL SCIENCES > 0301 Analytical Chemistry > 030108 Separation Science @ 50% |
| SEO Codes: | 97 EXPANDING KNOWLEDGE > 970103 Expanding Knowledge in the Chemical Sciences @ 100% |
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